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The Inorganic Analysis of Petroleum



 
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Product Code: 9780820603995

Description
 


ISBN-13/EAN: 9780820603995
ISBN: 0820603996
Author: James W. McCoy
Chemical Publishing
Book - Hardback
Pub Date: Sep 2, 1962
210 pages
Features


Although many papers have been published describing methods for the inorganic analysis of petroleum no book has previously appeared devoted exclusively to this subject.


The purpose of this work is to provide a laboratory handbook for industrial analysts of various degrees of professional training covering the determination of those elements commonly occurring in various types of petroleum products.


The procedures represent, from the author's point of view, a reasonable compromise among the usual conflicting interests of speed, accuracy, and cost, and emphasize manufacturing rather than research applications. 


"James McCoy"

Contents:

Introduction 
1. The Inorganic Components of Petroleum 
2. Preparation of Samples for Inorganic Analysis
Direct Ashing 
Soft Ashing and Wet Oxidation 
Direct Wet Oxidation 
Fusion with Pyrosulfate 
The Oxygen Bomb 
The Peroxide Bomb 
Sodium Dehalogenation 
Extraction Methods 
Combustion Methods 
Alkaline Sulfide Treatment 
Direct Methods 
Combustion Tube 
Emission Spectrograph 
X-rays 
3. Aluminum 
Colorimetric Determination 
Gravimetric Determination 
4. Arsenic 
5. Barium 
Determination in New Lubricating Oils 
Determination in Used Lubricating Oils 
6. Boron 
Colorimetric Determination 
Alkalimetric Determination 
7. Calcium 
Determination in New Lubricating Oils and Additives
Determination in Used Lubricating Oils
Estimation of Smaller Concentrations
8. Chromium
9. Cobalt
Electrolytic Determination
Volumetric Determination
10. Copper
Determination in Gasoline
Determination in Naphthenate Driers
Determination in Distillates
Determination in Used Lubricating Oils
11. The Halogens
Peroxide Bomb Combustion
Sodium Dehalogenation
Extraction Procedures
Wickbold Oxyhydrogen Combustion
Potentiometric Determination of Bromide and Chloride
Colorimetric Determination of Chloride
Volumetric Determination of Fluoride
12. Iron
Determination in Distillates
Determination in Used Lubricating Oils
Determination in Naphthenate Driers
Colorimetric Determination
Volumetric Determination
13. Lead
Determination in Naphthenate Driers
Determination in Light Distillates
Determination in Lubricating Oils
14. Manganese
15. Molybdenum
Determination in New Lubricating Oils
Determination in Used Lubricating Oils
16. Nickel
Determination in Distillates
Gravimetric Determination
17. Nitrogen
Determination of Total Nitrogen by Kjeldahl Method
Determination of Basic Nitrogen
Determination of Quaternary Ammonium Compounds
18. Phosphorus
Decomposition by Ashing in Presence of Zinc Oxide
Colorimetric Methods
Alkalimetric Determination of Phosphorus
19. Selenium
Colorimetric Determination 
Volumetric Determination
20. Silicon 
Determination in Synthetic Oils 
Determination of Silica in Used Lubricating Oils 
21. Sodium 
Decomposition of Sample by Direct Ashing 
Gravimetric Determination 
Determination by Flame Photometer
22. Sulfur
Determination by Peroxide Fusion Bomb
Determination by Wickbold Oxyhydrogen Combustion
23. Vanadium 
Determination in Distillates 
Determination in Fuel Oils 
Volumetric Determination 
24. Zinc 
Determination in Additives and Naphthenate Driers
Determination in New and Used Lubricating Oils
Potentiometric Determination 
Gravimetric Determination
Appendix
Wickbold Apparatus for Oxyhydrogen Combustion
Index


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