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Microdiffusion Analysis and Volumetric Error



 
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ISBN-13/EAN: 9780820601519
ISBN: 0820601519
Author: Edward Conway
Chemical Publishing
Book - Hardback
Pub Date: Jul 28, 1963
482 pages
Features

CONTENTS -

I. INTRODUCTORY -

PART I - APPARATUS AND PRINCIPLES USED IN MICRODIFFUSION ANALYSIS -

II. A STANDARD MICRO DIFFUSION APPARATUS OR 'UNIT' -  

III. FACTORS INFLUENCING THE ABSORPTION RATE FROM OUTER TO INNER CHAMBER WITH SPECIAL REFERENCE TO AMMONIA -  

IV. GENERAL PRINCIPLES GOVERNING THE ABSORPTION TIME IN MICRO DIFFUSION ANALYSIS -

V. PIPETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND THEIR DELIVERY ERRORS -

VI. MICRO-BURETTES (SUITABLE FOR USE WITH THE STANDARD UNITS) AND ERRORS INVOLVED IN THEIR USE -

VII. THE MICRODIFFUSION METHOD WITH END-POINT VOLUMES AROUND 20 CUBIC MILLIMETRES -

VII. COLORIMETRY IN THE MICRODIFFUSION METHODS -

PART II - DESCRIPTION OF METHODS WITH THE STANDARD UNITS -

A. VOLATILE BASES -
Aa. Ammonia Group -

IX. AMMONIA. GENERAL METHOD USING STANDARD ACID AS ABSORBENT -

X. AMMONIA. GENERAL METHOD (USING THE BORIC-HCL PROCEDURE) -

XI. SPECIAL FACTORS INFLUENCING THE RATE OF AMMONIA ABSORPTION -

XII. OTHER METHODS FOR DETERMINING THE ABSORBED AMMONIA IN THE MICRO DIFFUSION PROCEDURE -

XIII. AMMONIA. BIOLOGICAL DETERMINATIONS -

XIV. TOTAL NITROGEN (OVER 100 µg N). -

XV. TOTAL NITROGEN (UNDER 100 µg N) FURTHER PROCEDURE -

XVI. TOTAL NITROGEN (1 TO 0·1 µg N) -

XVII. UREA (BLOOD AND URINE) -

XVIII. UREA IN TISSUES -

XIX. ADENOSINETRIPHOSPHORIC ACID, ADENYLIC ACID, ADENOSINE, ETC. -

XX. NITRATE, NITRITE AND AMIDE NITROGEN -

XXI. AMIDES (continued). GLUTAMINE -

XXII. MONOAMINE OXIDASE AND HISTAMINASE IN TISSUES -
Ab. Amine Group -

XXIII. DETERMINATION OF VOLATILE AMINES -
B. VOLATILE ACIDS -
Ba. The Carbon Dioxide Group -

XXIV. CARBONATES AND BICARBONATE -

XXV. BLOOD GLUCOSE AND FERMENTABLE SUGAR IN NORMAL URINE -

XXVI. DETERMINATION OF CARBONIC ANHYDRASE -

XXVII. OXIDATION RATES OF ORGANIC SUBSTANCES WITH A STANDARD OXIDANT WITH APPLICATION TO DETERMINATION OF MINUTE AMOUNTS OF CALCIUM AS OXALATE -
Bb. 1 Volatile Fatty Acids -

XXVIII. ACETIC ACID AND OTHER LOWER FATTY ACIDS -

XXIX. ASSAY OF ACETYLCHOLINESTERASE -
Bc. Volatile Weak Inorganic Acids and Phenols -

XXX. CYANIDE, AZIDE, SULPHIDE, PHENOLS -
C. VOLATILE ALCOHOLS -

XXXI. METHANOL AND ISOPROPANOL GROUP -

XXXII. ETHANOL -

XXXIII. ETHANOL FROM URETHANE -

D. VOLATILE ALDEHYDES -
Da. Formaldehyde Group

XXXIV. FORMALDEHYDE -

XXXV. FORMALDEHYDOGENIC STEROIDS (PERIODIC ACID AS OXIDANT) -

XXXVI. FORMALDEHYDOGENIC STEROIDS (SODIUM BISMUTHATE AS OXIDANT) -

XXXVII. GLYCINE (FORMALDEHYDE PRODUCED BY NINHYDRIN OXIDATION) -
Db. Acetaldehyde Group

XXXVIII. ACETALDEHYDE (SEMICARBAZIDE ABSORPTION) -
 
XXXIX. ACETALDEHYDE FROM LACTIC ACID AND THREONINE WITH BISULPHITE ABSORPTION -

E. VOLATILE KETONES -

XL. ACETONE (INCLUDING A RAPID CLINICAL METHOD USING THE NESSLER SOLUTION) -

F. VARIOUS VOLATILE OXIDISING AND REDUCING SUBSTANCES -
Fa. The Halogens -

XLI. THE HALOGENS (INTRODUCTORY) -

XLII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO IODIDE) -

XLIII. CHLORIDE (BY OXIDATION TO CHLORINE AND ABSORPTION INTO FAST GREEN) -

XLIV. BROMIDE -

XLV. IODIDES AND HALOGEN MIXTURES -

XLVI. SERIAL DETERMINATION OF ORGANICALLY BOUND HALOGEN -

XLVII. VOLATILE HALOGENATED HYDROCARBONS (CHLOROFORM, TRICHLORETHYLENE AND CARBON TETRACHLORIDE) -
Fb. Carbon Monoxide -

XLVIII. CARBON MONOXIDE -

XLIX. A RAPID CLINICAL METHOD FOR CARBON MONOXIDE
DETERMINATION -

G. VOLATILE SUBSTANCES OF TOXICOLOGICAL INTEREST -

L. FELDSTEIN AND KLENDSHOJ'S SYSTEM FOR THE DETERMINATION OF VOLATILE POISONS BY MICRODIFFUSION -

H. OTHER MISCELLANEOUS APPLICATIONS OF THE MICRODIFFUSION PRINCIPLE -

LI. TOTAL MOLECULAR CONCENTRATION IN FLUID SAMPLES OF ABOUT 3-4 MILLIGRAMS -

LII. SEPARATION OF CRYSTALS AND' GUMS' BY MICRODIFFUSION -
QUALITATIVE MICRO-DIFFUSION ANALYSIS -

LIII. SOME CONSIDERATIONS ON QUALITATIVE MICRO-DIFFUSION ANALYSIS -  

PART III - THE ERROR OF VOLUMETRIC TITRATION -

LIV. INTRODUCTORY -

LV. THE VARIABLE GLASS ERROR -

LVI. THE TOTAL VARIABLE GLASS ERROR AND ITS CONTROL -

LVII. THE VARIABLE CHEMICAL ERROR IN TITRATION -

LVIII. THE RATIONALE OF MICRO TITRATION -

LIX. THE CONSTANT GLASS ERROR -

LX. THE CONSTANT CHEMICAL ERROR -

LXI. VOLUMETRIC ERROR IN KJELDAHL NITROGEN ANALYSES -

LXIII. UREA EXCRETION AS RENAL FUNCTION TEST -

REFERENCES -

INDEX OF SUBJECTS -

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